HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Azide → HCID 21537560, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Azide | HCID 33557 | — |
| Reactant | HCID 12231058 | HCID 12231058 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 21537560 | HCID 21537560 | — |
Reaction Steps
2-(2-Furyl)-4,6-dichloropyrimidine (m.p. 68° - 70°C.) was reacted with sodium azide in aqueous acetone to give 2-(2-furyl)-4-azido-6-chloropyrimidine (m.p. 117° - 119°C.) and this was then nitrated to give 2-(5-nitro-2-furyl)-4-azido-6-chloropyrimidine (m.p. 114° - 116°C.) which was, in turn, reacted with hydrazine hydrate in isopropanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03957766 |
| Source dataset | uspto-grants-1976_05 |
| ORD ID | ord-7923da08aca74ea7a0856989ec32b853 |
| Source note | uspto-grants-1976_05 |