HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoic acid, 2-hydroxy-3-methyl-, methyl ester → 1,4-Cyclohexanedimethanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoic acid, 2-hydroxy-3-methyl-, methyl ester | HCID 31835 | — |
| Reactant | HCID 178435161 | HCID 178435161 | — |
| Reactant | HCID 178516258 | HCID 178516258 | — |
| Solvent | Water | HCID 962 | — |
| Product | 1,4-Cyclohexanedimethanol | HCID 7735 | — |
Reaction Steps
100 g of polyethylene terephthalate fibres in 4 l of water are dyed with 1 g of the dyestuff prepared according to the above example, which has first been brought to a finely divided state in the presence of dispersing agents, the dyeing being carried out in the presence of 15 g of o-cresotic acid methyl ester as the carrier for 2 hours at 100°C and pH 4.5. A brilliant yellow-tinged pink dyeing is obtained, which is distinguished by good built-up and high fastness to washing, thermofixing, rubbing and light. A similar colouration is obtained if polyester fibres from 1,4-bis-(hydroxymethyl)-cyclohexane and therephthalic acid are used.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03957822 |
| Source dataset | uspto-grants-1976_05 |
| ORD ID | ord-021b5b7ff07b4032bd60bb4cc9b56c09 |
| Source note | uspto-grants-1976_05 |