Propargyl bromide → HCID 53764637, compound

HRID 1076734Notes

Reaction equation

[Br:1][C:2]1[C:3]([OH:13])=[C:4]([O:11][CH3:12])[CH:5]=[C:6]([CH:10]=1)[C:7]([OH:9])=[O:8].[CH2:14](Br)[C:15]#[CH:16]>>[CH2:16]([O:8][C:7](=[O:9])[C:6]1[CH:10]=[C:2]([Br:1])[C:3]([OH:13])=[C:4]([O:11][CH3:12])[CH:5]=1)[C:15]#[CH:14]

Participants

Reactant 2

HCID 7842Propargyl bromide

HCID 806125-Bromovanillic acid

Product 1

HCID 53764637HCID 53764637, compound

Procedure

By utilizing the procedure of Example 5, by reacting 5-bromovanillic acid with propargyl bromide, there is obtained 5-bromovanillic acid propargyl ester; M.P. 121-122°C.

Sources & evidence

ORD record: ord-27c13b9e20b844c7a6d2528597206563
Source dataset: uspto-grants-1976_05
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US03957833

Reaction notes

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