Propargyl bromide → HCID 54011312, compound

HRID 1076739Notes

Reaction equation

HRID 1076739 reaction equation
[CH3:1][CH:2]([O:9][C:10]1[CH:18]=[CH:17][C:13]([C:14]([OH:16])=[O:15])=[CH:12][C:11]=1[Cl:19])[CH2:3][CH2:4][CH2:5][CH:6]([CH3:8])[CH3:7].[CH2:20](Br)[C:21]#[CH:22]>>[CH2:22]([O:15][C:14](=[O:16])[C:13]1[CH:17]=[CH:18][C:10]([O:9][CH:2]([CH3:1])[CH2:3][CH2:4][CH2:5][CH:6]([CH3:7])[CH3:8])=[C:11]([Cl:19])[CH:12]=1)[C:21]#[CH:20]

Participants

3

Reactant 2

HCID 7842Propargyl bromideHCID 22749278HCID 22749278, compound

Product 1

HCID 54011312HCID 54011312, compound

Procedure

By utilizing the procedure of Example 8, by reacting p-[(1,5-dimethylhexyl)oxy]-3-chlorobenzoic acid with propargyl bromide, there is obtained 4-[(1,5-dimethylhexyl)oxy]-3-chlorobenzoic acid propargyl ester; nD26 = 1.5155.

Sources & evidence

ORD record
ord-a8ed75ddc0054d69b8c7a210df310935
Source dataset
uspto-grants-1976_05
Patent number
US03957833

Reaction notes

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