1-Bromopent-2-yne → HCID 22749300, compound

HRID 1076742Notes

Reaction equation

HRID 1076742 reaction equation
[CH3:1][CH:2]([O:9][C:10]1[CH:18]=[CH:17][C:13]([C:14]([OH:16])=[O:15])=[CH:12][CH:11]=1)[CH2:3][CH2:4][CH2:5][CH:6]([CH3:8])[CH3:7].Br[CH2:20][C:21]#[C:22][CH2:23][CH3:24]>>[CH2:20]([O:15][C:14](=[O:16])[C:13]1[CH:12]=[CH:11][C:10]([O:9][CH:2]([CH3:1])[CH2:3][CH2:4][CH2:5][CH:6]([CH3:7])[CH3:8])=[CH:18][CH:17]=1)[C:21]#[C:22][CH2:23][CH3:24]

Participants

3

Reactant 2

HCID 853991-Bromopent-2-yneHCID 22749290HCID 22749290, compound

Product 1

HCID 22749300HCID 22749300, compound

Procedure

By utilizing the procedure of Example 8, by reacting p-[(1,5-dimethylhexyl)oxy]benzoic acid with 1-bromo-2-pentyne, there is obtained p-[(1,5-dimethylhexyl)oxy]benzoic acid-2-pentynyl ester; nD24 = 1.5078.

Sources & evidence

ORD record
ord-401344a404154a1b976dc62be1ec79d6
Source dataset
uspto-grants-1976_05
Patent number
US03957833

Reaction notes

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