1-Bromo-3,7-dimethylocta-2,6-diene → 3-Methyl-4-[(3,7-dimethyl-2,6-octadienyl)oxy]benzoic acid methyl ester

HRID 1076745Notes

Reaction equation

HRID 1076745 reaction equation
[CH3:1][O:2][C:3](=[O:12])[C:4]1[CH:9]=[CH:8][C:7]([OH:10])=[C:6]([CH3:11])[CH:5]=1.Br[CH2:14][CH:15]=[C:16]([CH3:23])[CH2:17][CH2:18][CH:19]=[C:20]([CH3:22])[CH3:21]>>[CH3:1][O:2][C:3](=[O:12])[C:4]1[CH:9]=[CH:8][C:7]([O:10][CH2:14][CH:15]=[C:16]([CH3:23])[CH2:17][CH2:18][CH:19]=[C:20]([CH3:22])[CH3:21])=[C:6]([CH3:11])[CH:5]=1

Participants

3

Reactant 2

HCID 802281-Bromo-3,7-dimethylocta-2,6-dieneHCID 11240684Methyl 4-hydroxy-3-methylbenzoate

Product 1

HCID 543689263-Methyl-4-[(3,7-dimethyl-2,6-octadienyl)oxy]benzoic acid methyl ester

Procedure

By utilizing the procedure of Example 19, by reacting 3-methyl-4-hydroxybenzoic acid methyl ester with 1-bromo-3,7-dimethyl-2,6-octadiene, there is obtained 3-methyl-4-[(3,7-dimethyl-2,6-octadienyl)oxy]benzoic acid methyl ester; nD28 = 1.5248.

Sources & evidence

ORD record
ord-1ce7f40974a14a5eac370f04040a2ba1
Source dataset
uspto-grants-1976_05
Patent number
US03957833

Reaction notes

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