Propargyl bromide → HCID 54344377, compound

HRID 1076750Notes

Reaction equation

[CH3:1][CH:2]([S:9][C:10]1[CH:18]=[CH:17][C:13]([C:14]([OH:16])=[O:15])=[CH:12][CH:11]=1)[CH2:3][CH2:4][CH2:5][CH:6]([CH3:8])[CH3:7].[CH2:19](Br)[C:20]#[CH:21]>>[CH2:21]([O:15][C:14](=[O:16])[C:13]1[CH:12]=[CH:11][C:10]([S:9][CH:2]([CH3:1])[CH2:3][CH2:4][CH2:5][CH:6]([CH3:7])[CH3:8])=[CH:18][CH:17]=1)[C:20]#[CH:19]

Participants

Reactant 2

HCID 7842Propargyl bromide

HCID 22749288HCID 22749288, compound

Product 1

HCID 54344377HCID 54344377, compound

Procedure

By utilizing the procedure of Example 8, by reacting p-[(1,5-dimethylhexyl)thio]benzoic acid and propargyl bromide, there is obtained p-[(1,5-dimethylhexyl)thio]benzoic acid propargyl ester M.P. 130°-131°C/0.03 mmHg.

Sources & evidence

ORD record: ord-20adecd4d60044639d8021f95dc5fb6d
Source dataset: uspto-grants-1976_05
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US03957833

Reaction notes

Loading…