HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Sulfamic Acid → 2-Amino-4-methyl-5-nitrobenzenesulfonic acid
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Sulfamic Acid | HCID 5987 | — |
| Edukt | 4-Nitro-m-toluidine | HCID 11898 | — |
| Produkt | 2-Amino-4-methyl-5-nitrobenzenesulfonic acid | HCID 3016283 | — |
Reaktionsschritte
1 mol of 1-amino-3-methyl-4-nitrobenzene, 1,000 ml of one of the solvents indicated below, 198 g of sulphamic acid and the % by volume of catalyst indicated below are reacted analogously to Example 2. The yields of 1-amino-3-methyl-4-nitrobenzene-6-sulphonic acid obtained, and the reaction temperatures are indicated in the table which follows:
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US03957860 |
| Quelldatensatz | uspto-grants-1976_05 |
| ORD ID | ord-4b3b5b3bdf5f4a32a8bcb72c491fc38a |
| Quellennotiz | uspto-grants-1976_05 |