HCID 515388, compound → HCID 21538483, compound

HRID 1076824Notes

Reaction equation

HRID 1076824 reaction equation
[CH2:1]([N:5]([CH2:42][CH2:43][CH2:44][CH3:45])[CH2:6][CH2:7][CH2:8][NH:9][C:10]([C:12]1[CH:25]=[CH:24][C:23]2[O:22][C:21]3[C:16](=[CH:17][C:18]([C:26]([NH:28][CH2:29][CH2:30][CH2:31][N:32]([CH2:37][CH2:38][CH2:39][CH3:40])[CH2:33][CH2:34][CH2:35][CH3:36])=[O:27])=[CH:19][CH:20]=3)[C:15](=O)[C:14]=2[CH:13]=1)=[O:11])[CH2:2][CH2:3][CH3:4]>[Pd]>[CH2:37]([N:32]([CH2:33][CH2:34][CH2:35][CH3:36])[CH2:31][CH2:30][CH2:29][NH:28][C:26]([C:18]1[CH:19]=[CH:20][C:21]2[O:22][C:23]3[C:14](=[CH:13][C:12]([C:10]([NH:9][CH2:8][CH2:7][CH2:6][N:5]([CH2:1][CH2:2][CH2:3][CH3:4])[CH2:42][CH2:43][CH2:44][CH3:45])=[O:11])=[CH:25][CH:24]=3)[CH2:15][C:16]=2[CH:17]=1)=[O:27])[CH2:38][CH2:39][CH3:40]

Participants

3

Reactant 1

HCID 515388HCID 515388, compound

Product 1

HCID 21538483HCID 21538483, compound

Reagents, catalysts & solvents 1

HCID 23938PalladiumCatalyst

Procedure

An alcoholic solution of N,N'-bis(3-di-n-butylaminopropyl)-9-oxoxanthene-2,7-dicarboxamide, prepared in Example 3, can be used with a palladium catalyst to effect a hydrogenation to give N,N'-bis(3-di-n-butylaminopropyl)xanthen-2,7-dicarboxamide.

Sources & evidence

ORD record
ord-100b102d3d704658ae5652fc5b724cc8
Source dataset
uspto-grants-1976_05
Patent number
US03957986

Reaction notes

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