HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 10-Chloro-1,4,6,9-tetrahydro-4,6-dioxopyrido(3,2-g)quinoline-2,8-dicarboxylic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 12403020 | HCID 12403020 | — |
| Solvent | Water | HCID 962 | — |
| Product | 10-Chloro-1,4,6,9-tetrahydro-4,6-dioxopyrido(3,2-g)quinoline-2,8-dicarboxylic acid | HCID 72775 | — |
Reaction Steps
1.05 g. of the diester compound prepared in Example 6 is heated at reflux for 1 hour in 20 ml. of 5% sodium hydroxide. The mixture is cooled, 10 ml. of water added, and the pH adjusted to 3 with concentrated hydrochloric acid. The bright yellow diacid is collected by filtration. It has a melting point greater than 310° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03959289 |
| Source dataset | uspto-grants-1976_05 |
| ORD ID | ord-056abfa51d6948ad8aacb4dea06c4419 |
| Source note | uspto-grants-1976_05 |