HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxalyl chloride → HCID 18999946, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | 26395-06-2 | HCID 12939651 | — |
| Product | HCID 18999946 | HCID 18999946 | — |
Reaction Steps
reacting 5-methyl-2-oxohexanoic acid with at least a 10% excess of the stoichiometric amount of oxalyl chloride under anhydrous conditions at a temperature of 25° to 60° C. for from 40 to 60 hours to form 5-methyl-2-oxohexanoyl chloride;
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03959312 |
| Source dataset | uspto-grants-1976_05 |
| ORD ID | ord-3fc29eaeba9b426caa3ffa4feaf77891 |
| Source note | uspto-grants-1976_05 |