HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methane → HCID 54153729, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methane | HCID 297 | — |
| Reactant | HCID 22790403 | HCID 22790403 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 54153729 | HCID 54153729 | — |
Reaction Steps
Shake 13β-ethylgona-1,3,5(10),8,14-pentaene-3,17β-diol (0.28 g.) in benzene (35 cc.) with 10% palladised charcoal (300 mg.) in an atmosphere of hydrogen until 25 cc. of hydrogen has been absorbed. Filter off the catalyst, evaporate the solvent and recrystallize the residue from methanol to obtain the title product, m.p. 234°-8°; ultraviolet absorption peak at 280 mμ (ε 41,200).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03959322 |
| Source dataset | uspto-grants-1976_05 |
| ORD ID | ord-f655217528404e3d8967d4cc512568c5 |
| Source note | uspto-grants-1976_05 |