HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 68144428, compound → HCID 68145841, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 68144428 | HCID 68144428 | — |
| Solvent | HCID 86733486 | HCID 86733486 | — |
| Product | HCID 68145841 | HCID 68145841 | 53.6% |
Reaction Steps
Hydrolyze dl-13-ethyl-17β-hydroxy-17-(1-hydroxyethyl)-3-methoxygona-2,5(10)-diene (0.70 g) in hydrochloric acid-methanol-water. Recrystallize from ethyl acetate to obtain the title compound (0.36 g), m.p. 159°-164°; ultraviolet absorption peak at 240 mμ (ε15,230), infrared absorption peaks at 3.0 μ (strong), 6.05 μ.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03959322 |
| Source dataset | uspto-grants-1976_05 |
| ORD ID | ord-9e77c54bf3c04a849f8a71167163ecd7 |
| Source note | uspto-grants-1976_05 |