HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 16192610, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 2,6-Dichlorobenzaldehyde | HCID 6737 | — |
| Reactant | 3-Hydrazinyl-5-methyl-4H-1,2,4-triazol-4-amine--hydrogen chloride (1/1) | HCID 19021715 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 16192610 | HCID 16192610 | — |
Reaction Steps
To a solution of 5.25 g (0.032 mole) of 4-amino-3-hydrazino-5-methyl-1,2,4-triazole hydrochloride in 100 ml of 75 percent ethanol was added 5.6 g (0.032 mole) of 2,6-dichlorobenzaldehyde and 0.5 ml of concentrated hydrochloric acid. The mixture was stirred and heated at reflux for 16 hours. After cooling, the precipitate was collected and washed with chilled ethanol and ether. Yield: 7.0 g, m.p. 244°-245° (D).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03959476 |
| Source dataset | uspto-grants-1976_05 |
| ORD ID | ord-48388c1de42841a0b1b4a3f684f477dc |
| Source note | uspto-grants-1976_05 |