1-Benzyl-4-piperidone → HCID 12319421, compound

HRID 1077319Notes

Reaction equation

HRID 1077319 reaction equation
[CH3:1][O:2][CH:3]([C:13]1[CH:18]=[CH:17][C:16]([F:19])=[CH:15][CH:14]=1)[C:4]1[CH:9]=[CH:8][C:7]([O:10][CH3:11])=[CH:6][C:5]=1Br.[CH2:20]([N:27]1[CH2:32][CH2:31]C(=O)[CH2:29][CH2:28]1)[C:21]1[CH:26]=[CH:25][CH:24]=[CH:23][CH:22]=1>CCCCCCC>[CH2:20]([N:27]1[CH2:32][CH2:31][C:1]2([C:9]3[C:4](=[CH:5][CH:6]=[C:7]([O:10][CH3:11])[CH:8]=3)[CH:3]([C:13]3[CH:18]=[CH:17][C:16]([F:19])=[CH:15][CH:14]=3)[O:2]2)[CH2:29][CH2:28]1)[C:21]1[CH:26]=[CH:25][CH:24]=[CH:23][CH:22]=1

Participants

4

Reactant 2

HCID 192201-Benzyl-4-piperidoneHCID 12319474HCID 12319474, compound

Product 1

HCID 12319421HCID 12319421, compound

Reagents, catalysts & solvents 1

HCID 8900HeptaneSolvent

Procedure

By following the manipulative procedure described above in Example 45, 2-bromo-4'-fluoro-4-methoxybenzhydryl methyl ether and 1-benzyl-4-piperidone are reacted to produce a white solid, m.p. 86°-88°, form heptane.

Workup

  1. customare reacted
  2. customto produce a white solid, m.p. 86°-88°

Sources & evidence

ORD record
ord-604f354951d54126a2eaf777f8362eb7
Source dataset
uspto-grants-1976_05
Patent number
US03959475

Reaction notes

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