Dimethylamine → HCID 12361779, compound

HRID 1077343Notes

Reaction equation

HRID 1077343 reaction equation
[CH3:1][N:2]1[C:14]2[CH2:13][CH2:12][CH:11](OS(C3C=CC(C)=CC=3)(=O)=O)[CH2:10][C:9]=2[C:8]2[C:3]1=[CH:4][CH:5]=[CH:6][CH:7]=2.[CH3:26][NH:27][CH3:28]>>[CH3:26][N:27]([CH3:28])[CH:11]1[CH2:10][C:9]2[C:8]3[C:3](=[CH:4][CH:5]=[CH:6][CH:7]=3)[N:2]([CH3:1])[C:14]=2[CH2:13][CH2:12]1

Participants

3

Reactant 2

HCID 674DimethylamineHCID 12891854HCID 12891854, compound

Product 1

HCID 12361779HCID 12361779, compound

Procedure

Following the procedure described in Example 18 and using 36.2 g. of 9-methyl-3-tosyloxy-1,2,3,4-tetrahydrocarbazole and 250 ml. of dimetylamine there was otained 9.5 g. of 3-(dimethylamino)-9-methyl-1,2,3,4-tetraydrocarbazole in the form of its hydrochloride salt and which melted at >300°C.

Sources & evidence

ORD record
ord-717883c121854af2bbae052633c65968
Source dataset
uspto-grants-1976_05
Patent number
US03959309

Reaction notes

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