Acetate → Hexanoic acid, 2-ethyl-, nickel salt (1:?)

HRID 1077410Notes

Reaction equation

[Ni:1].[C:2]1([CH3:8])[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[C:9]([O-:12])(=[O:11])C>>[Ni:1].[CH2:2]([CH:7]([CH2:6][CH2:5][CH2:4][CH3:3])[C:9]([OH:12])=[O:11])[CH3:8]

Participants

Reactant 3

HCID 175Acetate

HCID 935Nickel

HCID 1140Toluene

Product 1

HCID 24231Hexanoic acid, 2-ethyl-, nickel salt (1:?)

Procedure

The concentration of nickel in the acetate solution is practically 1 ppm or more, preferably, 10 ppm or higher. In case of using a nonpolar solvent such as toluene for obtaining a solution of 2-ethyl hexanoic acid nickel, the oxide 13 is unnecessary and the solution can be directly formed on the amorphous silicon film.

Sources & evidence

ORD record: ord-f222c7f2bd3442fd9386cb8ad3795050
Source dataset: uspto-grants-1996_08
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05543352

Reaction notes

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