HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bicyclo[2.2.1]heptane-1-methanesulfonic acid, 7,7-dimethyl-2-oxo-, (1S)- → HCID 86749702, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bicyclo[2.2.1]heptane-1-methanesulfonic acid, 7,7-dimethyl-2-oxo-, (1S)- | HCID 18462 | — |
| Reactant | 6-(2-amino-indan-5-yl)-4,5-dihydropyridazin-3(2H)-one | HCID 14071499 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 86749702 | HCID 86749702 | — |
Reaction Steps
In 1,400 ml of ethanol was dissolved 8.41 g of 2-amino-5-[4,5-dihydropyridazin-3(2H)-on-6-yl]indane, and 8.52 g of (+)-camphorsulfonic acid was added to the solution. The resulting salts were recrystallized from ethanol several times to obtain 5.20 g of optically active 2-amino-5-[4,5-dihydropyridazin-3(2H)-on-6-yl]indane·(+)-camphorsulfonate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05543409 |
| Source dataset | uspto-grants-1996_08 |
| ORD ID | ord-e5d82262e72b4c8898a35498051ddb44 |
| Source note | uspto-grants-1996_08 |