HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(3,5-Dimethoxyphenyl)prop-2-enoic acid → 147700-47-8
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(3,5-Dimethoxyphenyl)prop-2-enoic acid | HCID 86092 | — |
| Reactant | 5,6-Diamino-1,3-dipropyl-2,4(1H,3H)-pyrimidinedione | HCID 5098605 | — |
| Product | 147700-47-8 | HCID 5379728 | 54.2% |
Reaction Steps
Substantially the same procedure as in Reference Example 1 was repeated using 3.95 g (17.5 mmol) of 5,6-diamino-1,3-dipropyluracil and 4.0 g (19.2 mmol) of 3,5-dimethoxycinnamic acid. Then, the resultant crude crystals were recrystallized from dimethylformamide/water to give 3.78 g (yield 54%) of Compound 33 as a white powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05543415 |
| Source dataset | uspto-grants-1996_08 |
| ORD ID | ord-1e5a43ad0d2e42249c917465a1d837c9 |
| Source note | uspto-grants-1996_08 |