HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(4-methoxynaphthyl)acrylic acid → 151539-63-8
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(4-methoxynaphthyl)acrylic acid | HCID 3880149 | — |
| Reactant | 5,6-Diamino-1,3-dipropyl-2,4(1H,3H)-pyrimidinedione | HCID 5098605 | — |
| Product | 151539-63-8 | HCID 6448812 | 56.1% |
Reaction Steps
Substantially the same procedure as in Reference Example 1 was repeated using 3.0 g (13.3 mmol) of 5,6-diamino-1,3-dipropyluracil and 3.33 g (14.6 mmol) of 3-(4-methoxynaphthyl)acrylic acid. Then, the resultant crude crystals were recrystallized from dioxane/water to give 3.12 g (yield 56%) of Compound 62 as yellow needles.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05543415 |
| Source dataset | uspto-grants-1996_08 |
| ORD ID | ord-2153a45285d74083b7be9aaa70db7368 |
| Source note | uspto-grants-1996_08 |