HuagongsheHuagongshe Chemistry Print Report · For research reference only
3',4'-Dimethoxycinnamic acid → 1H-Purine-2,6-dione, 3,7-dihydro-8-(2-(3,4-dimethoxyphenyl)ethenyl)-1,3-di-2-propenyl-, (E)-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3',4'-Dimethoxycinnamic acid | HCID 16848 | — |
| Reactant | 1,3-Diallyl-5,6-diaminouracil | HCID 13525062 | — |
| Product | 1H-Purine-2,6-dione, 3,7-dihydro-8-(2-(3,4-dimethoxyphenyl)ethenyl)-1,3-di-2-propenyl-, (E)- | HCID 6448972 | — |
Reaction Steps
Substantially the same procedure as in Reference Example 1 was repeated using 2.9 g (13.1 mmol) of 1,3-diallyl-5,6-diaminouracil and 2.99 g (14.4 mmol) of 3,4-dimethoxycinnamic acid. Then, the resultant crude crystals were recrystallized from dioxane/water to give 2.80 g (yield of Compound 69 as pale yellow flocculent precipitates.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05543415 |
| Source dataset | uspto-grants-1996_08 |
| ORD ID | ord-9b9782361a0c458fa7ef2204044086ab |
| Source note | uspto-grants-1996_08 |