HRID1077479

反应详情

EQUATION

反应方程式

HRID 1077479 的结构方程式

PROCEDURE

实验过程

Substantially the same procedure as in Reference Example 70 was repeated using 2.0 g (10.1 mmol) of 5,6-diamino-1,3-diethyluracil and 2.52 g (12.1 mmol) of 2,3-dimethoxycinnamic acid. Then, the resultant crude crystals were recrystallized from dimethylsulfoxide/water to give 1.72 g (yield 46%) of Compound 75 as a white powder.

WORKUP

后处理

  1. customThen, the resultant crude crystals were recrystallized from dimethylsulfoxide/water