돌아가기
Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 1077487생성일: 2026년 10월 26일

5,6-Diamino-1,3-dimethyluracil → 1H-Purine-2,6-dione, 3,7-dihydro-1,3-dimethyl-8-(2-(2,3,4-trimethoxyphenyl)ethenyl)-, (E)-

https://huagongshe.com/reaction/1077487

반응식

참여 물질

역할이름HCID투입량
반응물5,6-Diamino-1,3-dimethyluracilHCID 79501—
반응물3-(2,3,4-Trimethoxyphenyl)-2-propenoic acidHCID 118400—
생성물1H-Purine-2,6-dione, 3,7-dihydro-1,3-dimethyl-8-(2-(2,3,4-trimethoxyphenyl)ethenyl)-, (E)-HCID 644875035%

반응 단계

Substantially the same procedure as in Reference Example 70 was repeated using 5.00 g (29.4 mmol) of 5,6-diamino-1,3-dimethyluracil and 7.71 g (32.4 mmol) of 2,3,4-trimethoxycinnamic acid. Then, the resultant crude crystals were recrystallized from 2-propanol/water to give 3.78 g (yield 35%) of Compound 91 as an ocher powder.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US05543415
출처 데이터셋uspto-grants-1996_08
ORD IDord-3abac1e628d24f5183eb800fc8bafc2c
출처 메모uspto-grants-1996_08