huagongshe.com
HRID1077488

反应详情

EQUATION

反应方程式

HRID 1077488 的结构方程式

REACTANTS

反应物

2
结构：Cn1c(N)c(N)c(=O)n(C)c1=O
HCID79501

2,4(1H,3H)-Pyrimidinedione, 5,6-diamino-1,3-dimethyl-

C6H10N4O2

结构：COc1ccc(C=CC(=O)O)c(C)c1C
HCID53401770

3-(4-Methoxy-2,3-dimethylphenyl)-2-propenoic acid

C12H14O3

PRODUCTS

生成物

1
结构：COc1ccc(/C=C/c2nc3c([nH]2)c(=O)n(C)c(=O)n3C)c(C)c1C
HCID6448865

未命名化合物

收率 22%

PROCEDURE

实验过程

Substantially the same procedure as in Reference Example 70 was repeated using 1.74 g (10.2 mmol) of 5,6-diamino-1,3-dimethyluracil and 2.42 g (11.8 mmol) of 4-methoxy-2,3-dimethylcinnamic acid. Then, the resultant crude crystals were recrystallized from acetonitrile to give 750 mg (yield 22%) of Compound 93 as a white powder.

WORKUP

后处理

  1. customThen, the resultant crude crystals were recrystallized from acetonitrile