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HRID1077489

反应详情

EQUATION

反应方程式

HRID 1077489 的结构方程式

REACTANTS

反应物

2
结构：O=C(O)C=Cc1ccc2c(c1)OCO2
HCID16917

3',4'-Methylenedioxycinnamic acid

C10H8O4

结构：Cn1c(N)c(N)c(=O)n(C)c1=O
HCID79501

2,4(1H,3H)-Pyrimidinedione, 5,6-diamino-1,3-dimethyl-

C6H10N4O2

PRODUCTS

生成物

1
结构：Cn1c(=O)c2[nH]c(/C=C/c3ccc4c(c3)OCO4)nc2n(C)c1=O
HCID6062002

1H-Purine-2,6-dione, 8-[(1E)-2-(1,3-benzodioxol-5-yl)ethenyl]-3,7-dihydro-1,3-dimethyl-

C16H14N4O4

收率 13%

PROCEDURE

实验过程

Substantially the same procedure as in Reference Example 70 was repeated using 5.0 g (29.4 retool) of 5,6-diamino-1,3-dimethyluracil and 6.78 g (35.3 mmol) of 3,4-methylenedioxycinnamic acid. Then, the resultant crude crystals were recrystallized from dimethylformamide/water to give 1.20 g (yield 13%) of Compound 95 as a pale yellow powder.

WORKUP

后处理

  1. customThen, the resultant crude crystals were recrystallized from dimethylformamide/water