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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 1077490생성일: 2026년 10월 25일

5,6-Diamino-1,3-dimethyluracil → 1H-Purine-2,6-dione, 3,7-dihydro-8-(2-(2,3-dimethoxyphenyl)ethenyl)-1,3-dimethyl-, (E)-

https://huagongshe.com/reaction/1077490

반응식

참여 물질

역할이름HCID투입량
반응물5,6-Diamino-1,3-dimethyluracilHCID 79501—
반응물2,3-Dimethoxycinnamic acidHCID 99525—
생성물1H-Purine-2,6-dione, 3,7-dihydro-8-(2-(2,3-dimethoxyphenyl)ethenyl)-1,3-dimethyl-, (E)-HCID 5379232—

반응 단계

Substantially the same procedure as in Reference Example 70 was repeated using 2.50 g (14.7 mmol) of 5,6-diamino-1,3-dimethyluracil and 3.37 g (16.2 mmol) of 2,3-dimethoxycinnamic acid. Then, the resultant crude crystals were recrystallized from ethanol/water to give 1.03 g (yield of Compound 97 as pale yellow needles.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US05543415
출처 데이터셋uspto-grants-1996_08
ORD IDord-e326f5bdacc54f0ab5ee50ec6e3e2afd
출처 메모uspto-grants-1996_08