HuagongsheHuagongshe Chemistry Print Report · For research reference only
5,6-Diamino-1,3-dimethyluracil → 155271-50-4
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5,6-Diamino-1,3-dimethyluracil | HCID 79501 | — |
| Reactant | 3-(3-Bromo-4-methoxyphenyl)-2-propenoic acid | HCID 719754 | — |
| Product | 155271-50-4 | HCID 6448896 | 43.3% |
Reaction Steps
Substantially the same procedure as in Reference Example 70 was repeated using 2.00 g (11.8 mmol) of 5,6-diamino-1,3-dimethyluracil and 3.32 g (12.9 mmol) of 3-bromo-4-methoxycinnamic acid. Then, the resultant crude crystals were recrystallized from dimethylformamide to give 2.00 g (yield 43%) of Compound 115 as a pale yellow powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05543415 |
| Source dataset | uspto-grants-1996_08 |
| ORD ID | ord-b4f529cca1d145d68fd53b64da571593 |
| Source note | uspto-grants-1996_08 |