HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 3891318, compound → 1H-Purine-2,6-dione, 3,7-dihydro-1,3-diethyl-8-(2-(4-propoxyphenyl)ethenyl)-, (E)-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 3891318 | HCID 3891318 | — |
| Reactant | 5,6-Diamino-1,3-diethyluracil | HCID 4572133 | — |
| Product | 1H-Purine-2,6-dione, 3,7-dihydro-1,3-diethyl-8-(2-(4-propoxyphenyl)ethenyl)-, (E)- | HCID 6448876 | 54.3% |
Reaction Steps
Substantially the same procedure as in Reference Example 70 was repeated using 3.00 g (15.1 mmol) of 5,6-diamino-1,3-diethyluracil and 3.43 g (16.6 mmol) of 4-propoxycinnamic acid. Then, the resultant crude crystals were recrystallized from dioxane/water to give 3.02 g (yield 54%) of Compound 125 as pale yellow needles.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05543415 |
| Source dataset | uspto-grants-1996_08 |
| ORD ID | ord-ef89161fcd2e44e99d65d60153f6e8b1 |
| Source note | uspto-grants-1996_08 |