HRID1077504

反应详情

EQUATION

反应方程式

HRID 1077504 的结构方程式

PROCEDURE

实验过程

Substantially the same procedure as in Reference Example 70 was repeated using 3.00 g (15.1 mmol) of 5,6-diamino-1,3-diethyluracil and 2.77 g (16.7 retool) of 3-fluorocinnamic acid. Then, the resultant crude crystals were recrystallized from dioxane/water to give 1.96 g (yield 40% of Compound 127 as a pale yellow powder.

WORKUP

后处理

  1. customThen, the resultant crude crystals were recrystallized from dioxane/water