HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-[4-(Trifluoromethyl)phenyl]prop-2-enoic acid → 155271-66-2
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-[4-(Trifluoromethyl)phenyl]prop-2-enoic acid | HCID 74940 | — |
| Reactant | 5,6-Diamino-1,3-diethyluracil | HCID 4572133 | — |
| Product | 155271-66-2 | HCID 6448912 | 49.3% |
Reaction Steps
Substantially the same procedure as in Reference Example 70 was repeated using 2.20 g (11.2 mmol) of 5,6-diamino-1,3-diethyluracil and 2.66 g (12.3 mmol) of 4-trifluoromethyl-cinnamic acid. Then, the resultant crude crystals were recrystallized from dioxane/water to give 2.09 g (yield 49%) of Compound 135 as a white powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05543415 |
| Source dataset | uspto-grants-1996_08 |
| ORD ID | ord-d4e088b8486e4e54988828c3b25942b8 |
| Source note | uspto-grants-1996_08 |