HuagongsheHuagongshe Chemistry Print Report · For research reference only
5,6-Diamino-1,3-diethyluracil → 155271-74-2
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5,6-Diamino-1,3-diethyluracil | HCID 4572133 | — |
| Reactant | 3-[4-(Methoxymethoxy)phenyl]prop-2-enoic acid | HCID 54126028 | — |
| Product | 155271-74-2 | HCID 6448920 | 64.2% |
Reaction Steps
Substantially the same procedure as in Reference Example 70 was repeated using 4.00 g (20.2 mmol) of 5,6-diamino-1,3-diethyluracil and 4.62 g (22.2 mmol) of 4-methoxymethoxy-cinnamic acid. Then, the resultant crude crystals were recrystallized from dioxane/water to give 4.80 g (yield 64%) of Compound 145 as pale yellow needles.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05543415 |
| Source dataset | uspto-grants-1996_08 |
| ORD ID | ord-960947671d0648f280172d281790d1d9 |
| Source note | uspto-grants-1996_08 |