HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 735855, compound → 1H-Purine-2,6-dione, 3,7-dihydro-1,3-diethyl-8-(2-(3-phenoxyphenyl)ethenyl)-, (E)-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 735855 | HCID 735855 | — |
| Reactant | 5,6-Diamino-1,3-diethyluracil | HCID 4572133 | — |
| Product | 1H-Purine-2,6-dione, 3,7-dihydro-1,3-diethyl-8-(2-(3-phenoxyphenyl)ethenyl)-, (E)- | HCID 6448979 | — |
Reaction Steps
Substantially the same procedure as in Reference Example 70 was repeated using 3.00 g (15.1 mmol) of 5,6-diamino-1,3-diethyluracil and 4.00 g (16.7 mmol) of 3-phenoxycinnamic acid. Then, the resultant crude crystals were recrystallized from dioxane/water to give 3.82 g (yield of Compound 191 as pale yellow needles.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05543415 |
| Source dataset | uspto-grants-1996_08 |
| ORD ID | ord-44655bd9b3794b09b37388452935d554 |
| Source note | uspto-grants-1996_08 |