Methyl iodide → HCID 19075414, compound

HRID 1077722Notes

Reaction equation

HRID 1077722 reaction equation
[CH3:1][I:2].[CH2:3]([O:7][C:8]1[C:12]([C:13]2[CH:14]=[N:15][CH:16]=[CH:17][CH:18]=2)=[N:11][S:10][N:9]=1)[CH:4]([CH3:6])[CH3:5]>CC(C)=O>[I-:2].[CH2:3]([O:7][C:8]1[C:12]([C:13]2[CH:14]=[N+:15]([CH3:1])[CH:16]=[CH:17][CH:18]=2)=[N:11][S:10][N:9]=1)[CH:4]([CH3:6])[CH3:5]

Participants

4

Reactant 2

HCID 6328Methyl iodideHCID 19075496HCID 19075496, compound

Product 1

HCID 19075414HCID 19075414, compound

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

A mixture of methyl iodide (0.6 ml, 10 mmol) and 3-(3-isobutoxy-1,2,5-thiadiazol-4-yl)pyridine (588 mg, 2.5 mmol) in acetone (5 ml) was stirred at room temperature for 18 h. The title compound precipitated from the solution and was collected by filtration to yield 0.88 g (87%).

Workup

  1. customThe title compound precipitated from the solution
  2. filtrationwas collected by filtration
  3. customto yield 0.88 g (87%)

Sources & evidence

ORD record
ord-8ec80ec5d7444cee8cd97af997d88077
Source dataset
uspto-grants-1996_08
Patent number
US05545638

Reaction notes

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