Methyl iodide → HCID 19075288, compound

HRID 1077728Notes

Reaction equation

HRID 1077728 reaction equation
[CH3:1][I:2].[CH2:3]([O:10][C:11]1[C:15]([C:16]2[CH:17]=[N:18][CH:19]=[CH:20][CH:21]=2)=[N:14][S:13][N:12]=1)[C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][CH:5]=1>CC(C)=O>[I-:2].[CH2:3]([O:10][C:11]1[C:15]([C:16]2[CH:17]=[N+:18]([CH3:1])[CH:19]=[CH:20][CH:21]=2)=[N:14][S:13][N:12]=1)[C:4]1[CH:5]=[CH:6][CH:7]=[CH:8][CH:9]=1

Participants

4

Reactant 2

HCID 6328Methyl iodideHCID 19075281HCID 19075281, compound

Product 1

HCID 19075288HCID 19075288, compound

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

A mixture of methyl iodide (0.5 ml, 7.5 mmol) and 3-(3-benzyloxy-1,2,5-thiadiazol-4-yl)pyridine (673 mg, 2.5 mmol) in acetone (5 ml) was stirred at room temperature for 18 h. The title compound precipitated from the solution and was collected by filtration to yield 0.75 g (73%).

Workup

  1. customThe title compound precipitated from the solution
  2. filtrationwas collected by filtration
  3. customto yield 0.75 g (73%)

Sources & evidence

ORD record
ord-e30f6d60cb7649e0ba4f2272c649a930
Source dataset
uspto-grants-1996_08
Patent number
US05545638

Reaction notes

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