HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → cis-3-(3-(3-Hexenyloxy)-1,2,5-thiadiazol-4-yl)-1-methylpyridinium iodide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | cis-3-(3-(3-Hexenyloxy)-1,2,5-thiadiazol-4-yl)pyridine | HCID 70144893 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | cis-3-(3-(3-Hexenyloxy)-1,2,5-thiadiazol-4-yl)-1-methylpyridinium iodide | HCID 70144331 | — |
Reaction Steps
A mixture of methyl iodide (0,5 ml, 7.5 mmol) and cis-3-(3-(3-hexenyloxy)-1,2,5-thiadiazol-4-yl)pyridine (3 mmol) in acetone (5 ml) was stirred at room temperature for 18 h. The title compound precipitated from the solution and was collected by filtration to yield 0.9 g (46%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05545638 |
| Source dataset | uspto-grants-1996_08 |
| ORD ID | ord-f6e05a6e83ba4553aa5ec249a6930ea7 |
| Source note | uspto-grants-1996_08 |