Methyl iodide → HCID 19075355, compound

HRID 1077781Notes

Reaction equation

HRID 1077781 reaction equation
[CH3:1][I:2].[O:3]1[CH2:8][CH2:7][N:6]([C:9]2[C:13]([C:14]3[CH:15]=[N:16][CH:17]=[CH:18][CH:19]=3)=[N:12][S:11][N:10]=2)[CH2:5][CH2:4]1>CC(C)=O>[I-:2].[O:3]1[CH2:4][CH2:5][N:6]([C:9]2[C:13]([C:14]3[CH:15]=[N+:16]([CH3:1])[CH:17]=[CH:18][CH:19]=3)=[N:12][S:11][N:10]=2)[CH2:7][CH2:8]1

Participants

4

Reactant 2

HCID 6328Methyl iodideHCID 19075225HCID 19075225, compound

Product 1

HCID 19075355HCID 19075355, compound

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

A mixture of methyl iodide (0.5 ml, 8 mmol) and 3-(3-morpholino-1,2,5-thiadiazol-4-yl)pyridine (680 mg, 2.7 mmol) in acetone (5 ml) was stirred at room temperature for 18 h. The title compound precipitated from the solution and was collected by filtration to yield 1.0 g (94%).

Workup

  1. customThe title compound precipitated from the solution
  2. filtrationwas collected by filtration
  3. customto yield 1.0 g (94%)

Sources & evidence

ORD record
ord-f278e6786351428ca6ee6ed190158dec
Source dataset
uspto-grants-1996_08
Patent number
US05545638

Reaction notes

Loading…