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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1077796Generated: October 31, 2026

1-Butanol → HCID 15180173, compound

https://huagongshe.com/reaction/1077796

Reaction equation

Participants

RoleNameHCIDCharge
Reactant1-ButanolHCID 263—
ReactantSodiumHCID 5360545—
ReactantHCID 15180172HCID 15180172—
ProductHCID 15180173HCID 15180173—

Reaction Conditions

Temperature25 °C

Reaction Steps

To a solution of sodium (150 mg, 6.5 mmol) in 1-butanol (5 ml) was added 3-(3-chloro-1,2,5-oxadiazol-4-yl)pyridine (350 mg, 1.9 mmol). The mixture was stirred at 25° C. for 2 h and evaporated. The residue was dissolved in water and extracted with ether. The combined organic phases were dried and evaporated to give the title compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05545638
Source datasetuspto-grants-1996_08
ORD IDord-5a4221dbfb694b7687226d2a1aceec45
Source noteuspto-grants-1996_08