Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 1-Butanol | HCID 263 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | HCID 15180172 | HCID 15180172 | — |
| Product | HCID 15180173 | HCID 15180173 | — |
Reaction Steps
To a solution of sodium (150 mg, 6.5 mmol) in 1-butanol (5 ml) was added 3-(3-chloro-1,2,5-oxadiazol-4-yl)pyridine (350 mg, 1.9 mmol). The mixture was stirred at 25° C. for 2 h and evaporated. The residue was dissolved in water and extracted with ether. The combined organic phases were dried and evaporated to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US05545638 |
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| Source dataset | uspto-grants-1996_08 |
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| ORD ID | ord-5a4221dbfb694b7687226d2a1aceec45 |
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| Source note | uspto-grants-1996_08 |
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