HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 10478065, compound → HCID 54390555, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 10478065 | HCID 10478065 | — |
| Reactant | 5-Cyanopyridine-2-carboxylic acid | HCID 12400734 | — |
| Product | HCID 54390555 | HCID 54390555 | 47.8% |
Reaction Steps
Reaction of 2.5 g of t-butyl [[1-[3-(p-t-butoxyphenyl)-L-alanyl]-4-piperidinyl]oxy]acetate with 0.85 g of 5-cyano-2-picolinic acid (as in Example 1d) yields 1.55 g of t-butyl [[1-[3-(p-t-butoxyphenyl)-N-[[5-cyano-2-pyridyl]carbonyl]-L-alanyl]-4-piperidinyl]oxy]acetate. M.p. 122°-123° C. (diethyl ether/petroleum ether 4:1). MS (FAB): 565 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05545658 |
| Source dataset | uspto-grants-1996_08 |
| ORD ID | ord-5e50e8cd1d5b44dab7b347789dddec25 |
| Source note | uspto-grants-1996_08 |