Phenyl acetate → HCID 19430539, compound

HRID 1077983Notes

Reaction equation

[C:1]([O:4]C1C=CC=CC=1)(=[O:3])[CH3:2].C(O)(C1C=CC=CC=1)C1C=CC=CC=1.[F:25][C:26]([F:62])([F:61])[C:27]1[CH:28]=[C:29]([S:37]([NH:40][C:41]2[CH:56]=[C:55]([C:57]([F:60])([F:59])[F:58])[CH:54]=[CH:53][C:42]=2[O:43][C:44]2[CH:52]=[CH:51][CH:50]=[CH:49][C:45]=2C([O-])=O)(=[O:39])=[O:38])[CH:30]=[C:31]([C:33]([F:36])([F:35])[F:34])[CH:32]=1>>[F:35][C:33]([F:36])([F:34])[C:31]1[CH:30]=[C:29]([S:37]([NH:40][C:41]2[CH:56]=[C:55]([C:57]([F:59])([F:60])[F:58])[CH:54]=[CH:53][C:42]=2[O:43][C:44]2[CH:52]=[CH:51][CH:50]=[CH:49][C:45]=2[CH2:2][C:1]([OH:4])=[O:3])(=[O:38])=[O:39])[CH:28]=[C:27]([C:26]([F:61])([F:62])[F:25])[CH:32]=1

Participants

Reactant 2

HCID 31229Phenyl acetate

HCID 131719489Benzhydrol 2-[2-[3,5-bis(trifluoromethyl)phenylsulfonamido]-4-trifluoromethylphenoxy]benzoate

Product 1

HCID 19430539HCID 19430539, compound

Procedure

Following the procedure of Example 1(f) except substituting benzhydrol 2-[3,5-bis (trifluoromethyl)phenylsulfonamido]-4-trifluoromethylphenoxy]phenyl acetate for benzhydrol 2-[2-[3,5-bis(trifluoromethyl)phenylsulfonamido]-4-trifluoromethylphenoxy]benzoate, the title compound was obtained; mp 165°-166° C.

Sources & evidence

ORD record: ord-fc5eeb47ed024c5eb24558e9aab8a54d
Source dataset: uspto-grants-1996_08
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05545669

Reaction notes

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