HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diazomethane → HCID 19430584, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diazomethane | HCID 9550 | — |
| Reactant | 5-tert-amylsalicylic acid | HCID 268742 | — |
| Product | HCID 19430584 | HCID 19430584 | — |
Reaction Steps
Following the procedure of Schmitt et al., Synthesis, 1984, 758-760; and treating the resulting 2-hydroxy-5-(1,1-dimethylpropyl)benzoic acid with diazomethane gave the title compound. 1H NMR (250 MHz, CDCl3) δ10.61 (s, 1H), 7.-75 (d, 1H), 7.44 (dd, 1H), 6.92 (d, 1H), 3.95 (s, 3H), 1.61 (q, 2H), 1.26 (s, 6H), 0.67 (t, 3H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05545669 |
| Source dataset | uspto-grants-1996_08 |
| ORD ID | ord-17600ace505d43e3b8a56a5ff7e0f621 |
| Source note | uspto-grants-1996_08 |