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Phthalonitrile → Gallium phthalocyanine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Phthalonitrile | HCID 7042 | — |
| 反応物 | HCID 131719385 | HCID 131719385 | — |
| 溶媒 | Ethylene Glycol | HCID 174 | — |
| 生成物 | Gallium phthalocyanine | HCID 136138306 | — |
反応手順
31.8 parts of phthalonitrile, 10.1 parts of gallium trimethoxide and 150 ml of ethylene glycol were stirred under nitrogen atmosphere at 200° C. for 24 hours, and the product obtained was filtered. Then the product was washed with N,N-dimethylformamide and methanol successively, and dried to give 25.1 parts of gallium phthalocyanine.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05545733 |
| 出典データセット | uspto-grants-1996_08 |
| ORD ID | ord-77cc3d692a2e48d6b6625a27fe455e75 |
| 出典メモ | uspto-grants-1996_08 |