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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1078054Erstellt: 26. Oktober 2026

1,2-Dichloro-4-nitrobenzene → 2-Chloro-1-fluoro-4-nitrobenzene

https://huagongshe.com/reaction/1078054

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt1,2-Dichloro-4-nitrobenzeneHCID 7443—
EduktPotassium FluorideHCID 522689—
KatalysatorDistearyldimethylammonium chlorideHCID 7879—
Produkt2-Chloro-1-fluoro-4-nitrobenzeneHCID 6768869%

Reaktionsschritte

576 g (3 mol) of 3,4-dichloronitrobenzene, 58 g (0.1 mol) of distearyldimethylammonium chloride and 139 g (2.4 mol) of potassium fluoride were reacted analogously to Example 1. After filtering with suction, the residue was dissolved in water, the organic phase was separated off and the combined organic phases were fractionated. 289 g (69%, relative to potassium fluoride employed) of 3-chloro-4-fluoronitrobenzene were obtained.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS05545768
Quelldatensatzuspto-grants-1996_08
ORD IDord-e30add03b270414caea64b94a829809e
Quellennotizuspto-grants-1996_08