Borane → 1,5-Diphenylpentan-3-amine

HRID 1078101Notes

Reaction equation

HRID 1078101 reaction equation
[C:1]1([CH2:7][CH2:8][C:9](=[N:18]O)[CH2:10][CH2:11][C:12]2[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.B>>[NH2:18][CH:9]([CH2:10][CH2:11][C:12]1[CH:13]=[CH:14][CH:15]=[CH:16][CH:17]=1)[CH2:8][CH2:7][C:1]1[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1

Participants

3

Reactant 2

HCID 6331BoraneHCID 225565N-(1,5-diphenylpentan-3-ylidene)hydroxylamine

Product 1

HCID 153888741,5-Diphenylpentan-3-amine

Procedure

According to the procedure of Feuer and Braunstein (J. Org. Chem. 1969, 34, 1817), the resultant compound of Example 31 was treated with borane to give the desired compound.

Sources & evidence

ORD record
ord-3f51f9ce0aad40f293e58968dfa145b5
Source dataset
uspto-grants-1996_08
Patent number
US05545750

Reaction notes

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