HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-Iodosuccinimide → 2-Amino-5-iodo-4-methylnicotinonitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-Iodosuccinimide | HCID 120273 | — |
| Reactant | 2-Amino-4-methylpyridine-3-carbonitrile | HCID 10396887 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | 2-Amino-5-iodo-4-methylnicotinonitrile | HCID 11391265 | — |
Reaction Steps
This compound is prepared in a manner analogous to that of Step C of Example 4, using 8.3 grams (0.063 mole) of 2-amino-3-cyano-4-methylpyridine (prepared as in Step B of Example 4) and 14.2 grams (0.063 mole) of N-iodosuccinimide in 250 mL of N,N-dimethylformamide, yielding 2-amino-3-cyano-5-iodo-4-methylpyridine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05547954 |
| Source dataset | uspto-grants-1996_08 |
| ORD ID | ord-970a7f9d1b7b4db0be9229d0d224e815 |
| Source note | uspto-grants-1996_08 |