HCID 15069909, compound → HCID 15069918, compound
Reaction equation
C(C1NC2C3[C@@H]1C[C@@H]1C(C=3C=CC=2)=C[C@H](N)CN1CCC)C.[CH2:23]([CH:25]1[NH:39][C:38]2[C:40]3[C@@H:26]1[CH2:27][C@@H:28]1[C:33]([C:34]=3[CH:35]=[CH:36][CH:37]=2)=[CH:32][C@H:31]([NH:41][CH:42]=[O:43])[CH2:30][N:29]1[CH2:44][CH2:45][CH3:46])C>>[CH3:23][C:25]1[NH:39][C:38]2[C:40]3[C:26]=1[CH2:27][C@@H:28]1[C@@H:33]([C:34]=3[CH:35]=[CH:36][CH:37]=2)[CH2:32][C@H:31]([NH:41][CH:42]=[O:43])[CH2:30][N:29]1[CH2:44][CH2:45][CH3:46]Participants
3
Procedure
from 9,10-didehydro-2,3beta-dihydro-2-ethyl-6-n-propyl-8alpha-ergolinylamine the N-(9,10-didehydro-2,3beta-dihydro-2-ethyl-6-n-propyl-8alpha-ergolinyl)-formamide, yield 71%
Sources & evidence
- ORD record
- ord-f95f300e424a403094a0d621d37248ae
- Source dataset
- uspto-grants-1996_08
- Patent number
- US05547958
Reaction notes
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