HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 19429474, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 3-Chloro-2,2-dimethylpropanoyl chloride | HCID 61345 | — |
| Reactant | 4-Chlorobenzylamine | HCID 66036 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 19429474 | HCID 19429474 | — |
Reaction Steps
In a similar manner to Example 52b, 3-chloro-2,2-dimethylpropionyl chloride (27.4 g) in dichloromethane (100 ml) was added to 4-chlorobenzylamine (25.0 g) and triethylamine (24.6 ml) in dichloromethane (400 ml) to give 3-chloro-N-(4-chlorobenzyl)-2,2-dimethylpropionamide, m.p. 97°-98° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05547972 |
| Source dataset | uspto-grants-1996_08 |
| ORD ID | ord-e96c53e691344091b31d3194f8e94551 |
| Source note | uspto-grants-1996_08 |