HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → 8-bromo-N-[1-(4-chlorophenyl)-1-methylethyl]octanamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 8-bromooctanoyl Chloride | HCID 11402228 | — |
| Reactant | 2-(4-Chlorophenyl)propan-2-amine hydrochloride | HCID 45158337 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 8-bromo-N-[1-(4-chlorophenyl)-1-methylethyl]octanamide | HCID 19429518 | — |
Reaction Steps
1-(4-Chlorophenyl)-1-methylethylamine hydrochloride (4.0 g) was reacted with 8-bromooctanoyl chloride (4.7 g) in dichloromethane (50 ml) containing triethylamine (8.1 ml), in a similar manner to Example 52b, to give 8-bromo-N-[1-(4-chlorophenyl)-1-methylethyl]octanamide which was used directly in part c).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05547972 |
| Source dataset | uspto-grants-1996_08 |
| ORD ID | ord-59de9b6e0ff74be1aff75c66f897d0c9 |
| Source note | uspto-grants-1996_08 |