HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 19428112, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 19428115 | HCID 19428115 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 19428112 | HCID 19428112 | — |
Reaction Steps
To 5.37 g (0.0135 mol) of (±)-6-nitro-4-[3-(trifluoromethyl)benzoyl]-3,4-dihydro-2H-1,4-benzoxazine-3-ethanol dissolved in 80 ml of dichloromethane are added dropwise 4.85 ml (0.0675 mol) of thionyl chloride and the mixture is stirred, while being kept warm in a bath of hot water, for 5 h 30.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05550125 |
| Source dataset | uspto-grants-1996_08 |
| ORD ID | ord-0487fac787a148508565520f4011cd2c |
| Source note | uspto-grants-1996_08 |