1-(2-Methoxyphenyl)piperazine → HCID 19428160, compound

HRID 1078585Notes

Reaction equation

HRID 1078585 reaction equation
Cl[CH2:2][CH2:3][C:4]1[C:5](=[O:21])[O:6][C:7]2[C:14]([O:15][CH2:16][CH3:17])=[C:13]([O:18][CH2:19][CH3:20])[CH:12]=[CH:11][C:8]=2[C:9]=1[CH3:10].[CH3:22][O:23][C:24]1[CH:29]=[CH:28][CH:27]=[CH:26][C:25]=1[N:30]1[CH2:35][CH2:34][NH:33][CH2:32][CH2:31]1>>[CH2:19]([O:18][C:13]1[CH:12]=[CH:11][C:8]2[C:9]([CH3:10])=[C:4]([CH2:3][CH2:2][N:33]3[CH2:32][CH2:31][N:30]([C:25]4[CH:26]=[CH:27][CH:28]=[CH:29][C:24]=4[O:23][CH3:22])[CH2:35][CH2:34]3)[C:5](=[O:21])[O:6][C:7]=2[C:14]=1[O:15][CH2:16][CH3:17])[CH3:20]

Participants

3

Reactant 2

HCID 13461-(2-Methoxyphenyl)piperazineHCID 19428131HCID 19428131, compound

Product 1

HCID 19428160HCID 19428160, compoundYield 13%

Procedure

Process B; starting materials: 3-(2-chloroethyl)-7,8-diethoxy-4-methyl-2H-1-benzopyran-2-one (Example 33) and 1-(2-methoxyphenyl)piperazine; yield 13% of crude product.

Sources & evidence

ORD record
ord-81d452b323e34cfbb6b94cca1c241af9
Source dataset
uspto-grants-1996_08
Patent number
US05550129

Reaction notes

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