HuagongsheHuagongshe Chemistry Print Report · For research reference only
6,7-Dimethoxy-1,2,3,4-tetrahydroisoquinoline hydrochloride → HCID 10720718, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6,7-Dimethoxy-1,2,3,4-tetrahydroisoquinoline hydrochloride | HCID 6456035 | — |
| Reactant | HCID 10689980 | HCID 10689980 | — |
| Product | HCID 10720718 | HCID 10720718 | 12.1% |
Reaction Steps
The procedure of Example 3 is repeated using 3.3 g of α-(2-chloroethyl)-3,4-dimethoxy-α-[(4-methylphenyl)thio]benzeneacetonitrile and 1.14 g of 6,7-dimethoxy-1,2,3,4-tetrahydroisoquinoline hydrochloride. This affords 0.311 g of the desired product as a brown oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05550149 |
| Source dataset | uspto-grants-1996_08 |
| ORD ID | ord-891df845e1ed4b3ea30608b547640fda |
| Source note | uspto-grants-1996_08 |